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As seen, the column operates at lowest possible reflux ratio in thefirst time interval to remove methanol as much as possible. Thereflux ratio gradually increases in the 2nd and 3rd time intervalsto retain the reactants (especially water) in the reaction zone andto have further reaction and to meet the product specifications.The overall batch time gradually increases with product purity ofthe product, which is obvious. Increasing batch time also increasesconversion of limiting reactant.
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